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[ccp4bb]: scala



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I am having trouble to scale a data set processed by
mosflm using SCALA.  The mosaicity of the crystal was
very high and the oscillation angle for data
collection is smaller than the mosaicity so all the
reflections are partial.  The data were collected
using
Stanford Synchrotron at SLAC

Followed are the input file and error message.  Any
suggestions will be very much appreciated.

#!/bin/sh

scala hklin col12_145to189_sort.mtz \
      hklout  col12_145to189.sca  \
       << eof-scala
run 1 batch 1 to 45
title my protein crystal data
intensities partial
scales batch bfactor on rotation spacing 5 
resolution 100 3.5
anomalous off
eof-scala


error message
Working array size =          5



 Matrix of number of overlaps between rotation ranges
for each run,
  for reflection observations which will be used for
scaling
 Each group is labelled "run_number.range"

 Note that the number of ranges is one less than the
number of scale factors



 **** FATAL ERROR: no overlaps anywhere ****


 ====| WARNING WARNING WARNING WARNING WARNING  |====
       At least one part of data has no overlaps







 Initial scales for run     1
     1.0000



 No observations for parameter     1 run     1
 No observations for parameter     2 run     1
<B><FONT COLOR="#FF0000"><!--SUMMARY_BEGIN-->
 Scala:  *** No observations ***
 Times: User:       4.2s System:    1.7s Elapsed:   
0:07
</pre>
<!--SUMMARY_END--></FONT></B>
<B><FONT COLOR="#FF0000"><!--SUMMARY_BEGIN-->
</html>
<!--SUMMARY_END--></FONT></B>


Mary

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