scala problem

[Florence Vincent <florence@afmb.cnrs-mrs.fr>]

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Dear all,

I am a young crystallographer and I am running scala for the first
time...
I am trying to scale a data processed with denzo (1.12beta).
I defined two batches and I would like to put some resolution limits on
each of them.
First I ran scala like this :

scale:
scala hklin junk2.mtz hklout scaled.mtz << eof-scala
run 1 batch 1 to 55 
run 2 batch 101 to 155
title OBP pig complexed with pyrazine  
scales bfactor on  rotation spacing 5 ! smooth scaling
#scales bfactor off DETECTOR 1 1 rotation spacing 5 
cycles 20
intensities partials 
sdcorr  1.2  0.02
reject scale 3.
reject merge 3.
resolution 30 1.4
anomalous off
final  partials test 0.8 1.2 maxwidth 5
eof-scala

And in order to put the resolution limits, I ran scala like this :

scale:
scala hklin junk2.mtz hklout scaled.mtz << eof-scala
run 1 batch 1 to 55 
resolution run 1 low 2.5 high 1.4
run 2 batch 101 to 155
resolution run 2 low 30 high 2.2
title OBP pig complexed with pyrazine  
scales bfactor on  rotation spacing 5 ! smooth scaling
#scales bfactor off DETECTOR 1 1 rotation spacing 5 
cycles 20
intensities partials 
sdcorr  1.2  0.02
reject scale 3.
reject merge 3.
anomalous off
final  partials test 0.8 1.2 maxwidth 5
eof-scala

And there is no difference in the results...So I would like to know how
to define the resolution limits correctly.

Thanks in advance for your help
Flo



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*Florence VINCENT                
*Architecture et Fonction       
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